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Commit 3ab8711c authored by Rolf Niepraschk's avatar Rolf Niepraschk
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Umsetzung neues Layout; stärkere Modularisierung

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disseminate them, above all within the framework of legal and
industrial metrology. The PTB thus is on top of the metrological
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that the object calibrated is traceable to national standards.
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Recognition Arrangement (MRA) drawn up by the International Committee
for Weights and Measures (CIPM). Under the MRA, all participating
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\textbf{\Large Die Physikalisch-Technische Bundesanstalt} (PTB) in
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technische Oberbeh\"orde der Bundesrepublik Deutschland f\"ur das
Messwesen und Teile der Sicherheitstechnik. Die PTB geh\"ort zum
Dienstbereich des Bundesministeriums f\"ur Wirtschaft und Energie.
Sie erf\"ullt die Anforderungen an Kalibrier- und Pr\"uflaboratorien
auf der Grundlage der DIN EN ISO/IEC 17025.
Zentrale Aufgabe der PTB ist es, die gesetzlichen Einheiten in
\"Ubereinstimmung mit dem Internationalen Einheitensystem (SI)
darzustellen, zu bewahren und -- insbesondere im Rahmen des
gesetzlichen und industriellen Messwesens -- weiterzugeben. Die PTB
steht damit an oberster Stelle der metrologischen Hierarchie in
Deutschland. Kalibrierscheine der PTB dokumentieren die
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highest technical authority of the Federal Republic of Germany for the
field of metrology and certain sectors of safety engineering. The PTB
comes under the auspices of the Federal Ministry of Economics and Energy.
It meets the requirements for calibration and testing
laboratories as defined in the EN ISO/IEC 17025.
It is fundamental task of the PTB to realize and maintain the legal
units in compliance with the International System of Units (SI) and to
disseminate them, above all within the framework of legal and
industrial metrology. The PTB thus is on top of the metrological
hierarchy in Germany. Calibration certificates issued by it document
that the object calibrated is traceable to national standards.
This certificate is consistent with Calibration and Measurement
Capabilities (CMCs) that are included in Appendix C of the Mutual
Recognition Arrangement (MRA) drawn up by the International Committee
for Weights and Measures (CIPM). Under the MRA, all participating
institutes recognize the validity of each other's calibration and
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%---------------------------
\listfiles
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\resultTable{ 6 }{%
{\(p_{cal}\)}&{\(p_{ind}\)}&{\(p_r\)}&{\(p_{ind} - p_r\)}&{\(e\)}&{\(U(k=2)\)}\\
mbar&mbar&mbar&mbar&&\\\toprule\endhead
2.954E-08&3.27E-08&1.66E-09&3.10E-08&5.1E-02&2.6E-02\\
4.970E-08&5.35E-08&1.65E-09&5.19E-08&4.3E-02&2.4E-02\\
8.908E-08&9.53E-08&1.63E-09&9.37E-08&5.2E-02&2.4E-02\\
2.991E-07&3.17E-07&1.68E-09&3.15E-07&5.4E-02&2.4E-02\\
4.805E-07&5.29E-07&1.80E-09&5.27E-07&9.7E-02&2.4E-02\\
4.810E-07&5.29E-07&2.00E-09&5.27E-07&9.6E-02&2.4E-02\\
5.024E-07&5.30E-07&1.80E-09&5.28E-07&5.1E-02&2.4E-02\\
8.916E-07&9.37E-07&1.52E-09&9.35E-07&4.9E-02&2.2E-02\\
2.943E-06&3.07E-06&1.77E-09&3.07E-06&4.3E-02&2.2E-02\\
4.922E-06&5.13E-06&2.02E-09&5.13E-06&4.2E-02&2.2E-02\\
8.827E-06&9.25E-06&3.20E-09&9.24E-06&4.7E-02&2.2E-02\\
2.957E-05&3.05E-05&4.10E-09&3.05E-05&3.1E-02&2.2E-02\\
4.892E-05&5.01E-05&6.70E-09&5.01E-05&2.4E-02&2.2E-02\\
8.768E-05&8.87E-05&7.70E-09&8.87E-05&1.1E-02&2.2E-02\\
8.960E-05&8.88E-05&1.20E-08&8.88E-05&-9.1E-03&2.2E-02\\
8.768E-05&8.88E-05&1.00E-08&8.88E-05&1.3E-02&2.2E-02\\
}
\missingEntries{ 16 }
\object{ Stabil Ion Gauge }
\manufacturer{ Granville-Phillips }
\type{ EXT-Y, Stabil Ion Controler 370B }
\serialNo{ YEA06800, 1449 }
\applicant{ { BOC EDWARDS } { Marshall Road } { EASTBOURNE, EAST SUSSEX } { BN22 9BA } }
\refNo{ ? }
\calibMark{ 75120 PTB 13 }
\calibDate{ 2013-11-26 }
\byOrder{ Dr. K. Jousten }
\examiner{ ? }
\certificateDate{ 2013-12-18 }
\begin{document}
\printFirstPage
\section{ Description of the calibration device }
%\num{9.99E-7 +- 9E-9} \par \bigskip
\num{9.99 +- 0.09} \par \bigskip
The device was shipped under atmospheric pressure kept in the producers plastic shell.
A memory module belonging to the stabil ion gauge (serial 06800) was provided. It was active during calibration.
\section{ Calibration procedure }
The device was installed in a vertical orientation. Before calibration the gauge head was baked at \(?\) °C for \(?\) h. During the cool down phase the head was degassed for \(?\) minutes. At room temperature it was exposed for \(?\) h at \(?⋅10^{?}\) mbar argon for sputtering the ion collector.
The sensitivity factor was kept at an value of \(?\) mbar\(^{-1}\) during the calibration. The calibration was carried out with the following device settings:
\begin{itemize}\item display: mbar\item filament: F1\item emission: L\item channel: A\end{itemize}
Before each calibration point the residual pressure indication \(p_r\) was checked.
The temperature \(θ\) during the calibration was \(?\) °C and varied from this value within \(\pm?\) °C.
The device was calibrated with ? in the pressure range \(?⋅ 10^{?}\) mbar to \(?⋅10^{?}\) mbar by comparing its reading with the calibration pressure that was established by the primary standard CE3 of PTB applying the continuous expansion method.
\section{ Relative error of indication }
The correction factor \(CF\) given in the table below was calculated from the indicated pressure \(p_{ind}\) as follows:\[CF =\frac{p_{cal}}{p_{ind} - p_{r}}\] where \(p_{cal}\) denotes the calibration pressure as generated in the primary standard and \(p_{r}\) the reading at residual pressure. From this, the corrected pressure \(p\) can be calculated from the residual pressure indication and the indicated pressure by:\[p = CF (p_{ind} - p_{r})\]
The uncertainty \(U\) of \(CF\) at the time of calibration is given in the last column of the table below. It includes the repeatability of \(p_{ind}\) for otherwise identical conditions (\(p_{cal}\), \(θ\)).\printResultTable
\section{ Uncertainty of Calibration }
The uncertainty \(U\) stated is the expanded measurement uncertainty obtained by multiplying the standard measurement uncertainty by the coverage factor \(k = 2\). It has been determined in accordance with the “Guide to the Expression of Uncertainty in Measurement (GUM)”. The value of the measurand then normally lies, with a probability of approximately \(95\) \%. within the attributed coverage interval.\par \(95\)\,\% 95\,\% 95~\% \(95\) \% \par
95 \% 95 \%
\printLastPage
\end{document}
%---------------------------
\(95\)\,\% 95\,\% 95~\%
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